STUDY OF THE DIFFUSION ELECTROLYTE PLASMA TREATMENT EFFECT ON THE TRIBOLOGICAL CHARACTERISTICS OF 40Kh STEEL
https://doi.org/10.53360/2788-7995-2025-3(19)-54
Abstract
This article studies the effects of diffusion electrolytic plasma boriding on the structure and tribological characteristics of 40Kh steel. X-ray diffraction and scanning microscopy were used to investigate the structural and phase composition, while the mechanical and tribological properties of the steel were measured using a hardness tester and tribometer. The characteristics of 40Kh steel in its initial state and after diffusion electrolytic plasma treatment followed by oxide removal by electrochemical polishing were compared. After diffusion electrolytic-plasma treatment, FeB and Fe₂B boride phases were detected on X-ray diffractograms, proving the diffusion process. A 5 times increase in microhardness and a 3 times decrease in wear intensity were also determined, depending on the initial state. It was established that the morphology of the structure after boriding has a zonality consisting of three zones: the borided layer, the diffusion zone, and the heat-affected zone. The research data indicates the potential of using diffusion electrolytic-plasma treatment in mechanical engineering and the processing of parts for the mining industry.
About the Authors
L. G. SulyubayevaKazakhstan
Laila Gylimmeddenovna Sulyubayeva – PhD, associate professor, Senior Researcher of Scientific Research Center «Surface Engineering and Tribology»
070002, Kazakhstan, Ust-Kamenogorsk, st. Shakarima 148
N. E. Berdimuratov
Kazakhstan
Nurbol Erboluly Berdimuratov – Junior researcher of scientific research center «Surface engineering and tribology»
070002, Kazakhstan, Ust-Kamenogorsk, st. Shakarima 148
T. Alimbekuly
Kazakhstan
Temirlan Alimbekuly – junior researcher of Scientific Research Center «Surface Engineering and Tribology»
070002, Kazakhstan, Ust-Kamenogorsk, st. Shakarima 148
References
1. Metal surface modification by plasma boronizing in a two-temperature-stage process / K.-S. Nam et al // Surface and Coatings Technology. – 2005. – № 197(1). – R. 51-55. https://doi.org/10.1016/j.surfcoat.2004.10.099. (In English).
2. Belkin P.N. Elektrolitno-plazmennoe borirovanie staley i titanovykh splavov: Obzor [Electrolyteplasma boriding of steels and titanium alloys: A review] / P.N. Belkin, A.A. Karpov, A.S. Pavlenko // Surface Engineering and Applied Electrochemistry. – 2022. – № 58(3). – R. 234-248. (In Russian).
3. Krivezhenko D.S. (2022). Razrabotka i issledovanie boridnykh pokrytii dlya uvelicheniya iznosostoykosti detaley iz stali. PhD Dissertation, MISIS, Moscow. (In Russian).
4. Malushin Y.T.I. Structural features and properties of boride coatings formed by electrolytic plasma processing / Y.T.I. Malushin // Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques. – 2020. – № 14(2). – R. 378-386. https://doi.org/10.1134/S102745102002019X. (In English).
5. Gunes I. An overview of boriding and recent developments in boride layer growth mechanisms / I. Gunes, F. Yildiz // Kovove Mater. – 2011. – № 49(2). – R. 95-102. (In English).
6. Kusmanov S.A. Teoreticheskie osnovy ehlektrolitno-plazmennogo nagreva i ego primenenie dlya diffuzionnogo nasyshcheniya metallov i splavov / S.A. Kusmanov, I.G. D'yakov, P.N. Belkin; Kostroma: Izd-vo Kostrom. gos. un-ta, 2017. – 420 s. (In Russian).
7. Medvedovski E. Wear and corrosion-resistant ceramic coatings for aggressive service conditions / E. Medvedovski // Surface and Coatings Technology. – 2015. – № 266. – R. 197-208. https://doi.org/10.1016/j.surfcoat.2015.01.011. (In English).
8. Korzec M.D. Plasma Electrolytic Saturation with Boron in Steel Surfaces / M.D. Korzec, K. Dybowski // Surface and Coatings Technology. – 1994. – № 63(1). – R. 53-58. https://doi.org/10.1016/S0257-8972(05)80006-1. (In English).
9. Pat. 10575. Respublika Kazakhstan. Sposob ehlektrolitno-plazmennogo borirovaniya stal'nykh izdelii v rasplave. / L.G. Sulyubaeva, N.E. Berdіmuratov, D.R. Baizhan, A.B. Nabioldina, Temіrlan Әlіmbekұly. Data reg.: 16.05.2025. (In Russian).
10. Ehlektrolitno-plazmennaya poverkhnostnaya zakalka nizkolegirovannykh stalei 65G i 20GL / B.K. Rakhadilov i dr. // Vestnik Karagandinskogo universiteta. – 2016. – № 4(84). – S. 8-13. (In Russian).
11. Rakhadilov B.K., Tabiyeva Y.Y., Uazyrkhanova G.K., Zhurerova L.G., Popova N.A. Effect of electrolyte-plasma surface hardening on structure wheel steel 2 // Bulletin of the Karaganda university. Physics series -2020. No.2(98) -P. 68-74 DOI 10.31489/2020Ph2/68-74. (In English).
12. Investigation of Changes in the Structural-Phase State and the Efficiency of Hardening of 30CrMnSiA Steel by the Method of Electrolytic Plasma Thermocyclic Surface Treatment / D. Baizhan et al // Coatings. – 2022. – V.12. https://doi.org/10.3390/coatings12111696. (In English).
13. Skakov M. Influence of Regimes Electrolytic Plasma Cementation on the Mechanical Properties of Steel 12Cr18Ni10Ti / M. Skakov, Sh. Kurbanbekov, M. Scheffler // Key Engineering Materials. – 2013. – V. 531-532. – P.173-177. https://doi.org/10.4028/www.scientific.net/KEM.531-532.173. (In English).
14. Change in high-temperature wear resistance of high-speed steel by plasma nitriding / B.K. Rakhadilov et al // Vestnik Karagandinskogo universiteta. – 2018. – № 3(91). – P. 59-65. (In English).
15. Dossett J.L. ASM handbook / J.L. Dossett, G.E. Totten // Heat Treating of Irons and Steels, ASM International, Materials Park, OH, USA. – 2014. – Vol. 4D. (In English).
16. Fazovye prevrashcheniya v stali 30KHGS pod deistviem ehlektrolitno-plazmennoi nitrotsementatsii / N.A. Popova i dr. // Vestnik Tomskogo gosudarstvennogo universiteta. –2016. – № 1. – S. 60-70. (In English).
17. Skakov M.K. Tekhnologiya Plazmenno-Ehlektroliticheskogo Borirovaniya Poverkhnosti Stali 30KHGSA / M.K. Skakov, EH.G. Batyrbekov, L.G. Zhurerova // Vestnik KaZNTU. – 2015. – № 3. – S. 377-384. (In Russian).
Review
For citations:
Sulyubayeva L.G., Berdimuratov N.E., Alimbekuly T. STUDY OF THE DIFFUSION ELECTROLYTE PLASMA TREATMENT EFFECT ON THE TRIBOLOGICAL CHARACTERISTICS OF 40Kh STEEL. Bulletin of Shakarim University. Technical Sciences. 2025;(3(19)):481-489. https://doi.org/10.53360/2788-7995-2025-3(19)-54















